Technical Column | Physical Examination for Composite Materials (II) – Compression Test

Introduction to Compression Testing

In our previous article, we introduced the tensile test, the primary method for evaluating the mechanical properties of composite materials.To further test a composite material’s ability to resist collapse and maintain structural stability under compressive loading, another test method is required: the compression test.

Composite compression testing is one of the more challenging tests, as the thin-walled structure of composite materials tends to experience buckling during actual testing rather than genuine material failure.Therefore, the key to compression testing is to prevent the load applied to the specimen from causing buckling.

① Buckling: Structural buckling refers to the phenomenon where a component loses its load-bearing capacity due to instability before reaching the yield strength of the material, characterized by a sudden deviation from its original equilibrium state.

I. Commonly Used Standards

At present, due to the wide variety of composite materials, their compression tests are conducted in accordance with many different standard systems.

Examples of national standards in China include: GB/T 34559-2017 Test Method for Compressive Properties of Carbon/Carbon Composites;

GB/T 33614-2017 Test Method for Compressive Properties of Three-Dimensional Braided Fabrics and Their Resin Matrix Composites;

GB/T 41955-2022 Test Method for Open-Hole-Free Compression of Multidirectional Polymer Matrix Composite Laminates, among others.

International standards include ISO 14544:2025 Ceramic composites — Mechanical properties at elevated temperatures — Determination of compressive properties and ISO 14126:2023 Fibre-reinforced plastic composites — Determination of compressive properties in the in-plane direction.

Standards from ASTM International include ASTM D6641 Standard Test Method for Compressive Properties of Polymer Matrix Composite Laminates Using a Combined Loading Compression (CLC) Test Grip and ASTM D3410 Standard Test Method for Compressive Properties of Polymer Matrix Composite Materials with Unsupported Gage Section, among others.

In addition to the above standards, many countries such as Germany, the United Kingdom and France have developed their own standard methods for compression tests of composite materials. Internationally, ASTM D6641 and ASTM D3410 are generally recognized as commonly used standards for compression testing.

II. Standard Differences

Although all the standards listed above can be used as references for composite material compression tests, it can be seen from their titles that each standard has a different emphasis.

Taking the commonly used ASTM D6641 Standard Test Method for Compressive Properties of Polymer Matrix Composite Laminates Using a Combined Loading Compression (CLC) Test Grip and ASTM D3410 *Standard Test Method for Compressive Properties of Polymer Matrix Composite Materials with Unsupported Gage Section as examples, the core difference between the two standards lies in the loading methods during testing: ASTM D6641 adopts a combined loading mode of “end loading + shear loading”, whereas ASTM D3410 employs pure shear loading.

Figure 1: Schematic Diagram of Pure Shear Loading Principle for ASTM D3410

Figure 1: Schematic Diagram of Pure Shear Loading Principle for ASTM D3410

 

The combined loading mode of ASTM D6641 not only minimizes specimen end crushing during testing but also reduces the influence of shear stress concentration, ensuring a uniform stress state.

This method is applicable for compressive property testing of high-strength, high-modulus continuous fiber-reinforced composites, especially unidirectional laminates and laminated plates, and features a wide range of material applicability.

ASTM D6641 is primarily used to determine the following properties:

  1. Compressive strength: the maximum compressive stress a specimen can withstand during a compression test.
  2. Compressive (elastic) modulus: the slope of the stresscompression curve over a specified strain interval within the elastic region.
  3. Strain at maximum load or failure strain: the compressive strain at which compressive strength is reached.
  4. Yield performance (if applicable): the stress value at which the composite material begins to undergo plastic deformation.
  5. Poisson’s ratio: the negative ratio of transverse strain to axial strain under uniaxial loading, used to characterize the lateral contraction or expansion behavior of the material (obtaining this parameter is not a mandatory requirement of ASTM D6641).

The pure shear loading mode of ASTM D3410 completely eliminates end loading during testing, making it suitable for high-performance composite materials sensitive to end failure. This method is specifically designed to determine the in-plane compressive properties of high-modulus fiber-reinforced polymer matrix composites.

This method can be used to measure the following material properties: ultimate compressive strength, ultimate compressive strain, compressive elastic modulus, compressive chord modulus, compressive Poisson’s ratio, transition strain, and secant modulus.

III. Common Precautions

Testing Equipment

For compression tests conducted on standard specimens in accordance with ASTM D6641 and ASTM D3410, as well as many other standardized test methods for fiber-reinforced plastics, a 100 kN to 300 kN electronic universal testing machine is generally sufficient.

SINOTEST provides an advanced solution suite for the performance testing of composite materials.

Figure 2: SINOTEST Composite Material Tensile Testing Solution
Figure 2: SINOTEST Composite Material Tensile Testing Solution

The solution adopts the SINOTEST DF Series Electronic Universal Testing Machine, which can perform composite material tensile tests in accordance with GB, ASTM, ISO and other industrial standards, featuring industry-leading accuracy and reliability.

  • Strong compatibility: Capable of meeting composite material tests of various types and standards.
  • Modular design: Allows quick replacement of composite material grips to adapt to test conditions under different standards.
  • High precision: Achieves Class 0.5 measurement accuracy.
  • Custom grip adaptability: Can be equipped with non-standard grips for composite specimens of special dimensions.
  • Wide speed range of the mainframe: Satisfies most test speed requirements.

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Stress-Compression Curve

Figure 3: Stress-Compression Curve Generated by SINOTEST Solution in Accordance with ASTM D6641

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Force-Time Curve

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Stress-Strain Curve

Figure 4: Test Curve Obtained by SINOTEST Solution in Accordance with ASTM D3410

Grip Selection

When conducting compression tests on composite specimens, appropriate grips shall be selected according to different standards.

For example, ASTM D6641 specifies the use of Combined Loading Compression (CLC) grips to achieve combined “end loading + shear loading”.

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Figure 5: Combined Loading Compression (CLC) grip

 ASTM D3410 requires the use of IITRI Grips, which convert the axial force applied by the testing machine platens into shear force on the parallel section (gauge section) of the specimen via internal wedges, thereby achieving pure shear loading.

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Figure 6: IITRI Grip

 SINOTEST offers a variety of modular grips for composite material compression testing, suitable for testing requirements involving multiple force levels and temperature ranges.

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Figure 7: SINOTEST Special Grip for ASTM D6641
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        Figure 8: SINOTEST Special Grip for ASTM D3410

Specimen Preparation

Requirements for specimens vary across standards, and specimens shall be prepared in accordance with specific standard provisions.

For instance, ASTM D6641 requires specimens to be rectangular laminated strips with or without tabs. The width shall be at least 13 mm, and the thickness must be sufficient to prevent Euler column buckling, while meeting specified dimensional and tolerance requirements.

Conclusion

This article presents the compression test methods for composite material performance testing in accordance with two ASTM standards. In the next issue of SINOTEST Composite Materials Series, we will elaborate on the relevant content of composite material flexural tests, and look forward to continuing our journey with you.

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